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Abstract
This research examines the synthesis of MIL-53(Al) through both conventional hydrothermal synthesis (MIL-53(Al)-C) and microwave-assisted (MIL-53(Al)-MW) techniques, revealing notable disparities in their morphology and adsorption characteristics. The microwave method produces small, more uniform particles with increased BET surface area compared to conventional methods. MIL-53(Al)-MW demonstrates elevated H2 uptake in the low-pressure range. These results underscore the impact of microwave-assisted synthesis compared to conventional techniques.
Supplementary materials
Title
Supplementary information
Description
The supplementary information includes additional details on the chemical, synthesis of MOF, characterization techniques, and results that are not provided in the main manuscript. These encompass Powder X-ray Diffraction (PXRD), Scanning Electron Microscopy (SEM), Thermogravimetric Analysis (TGA), Nitrogen Sorption, and High-Pressure Hydrogen Sorption measurements.
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