Catalytic synthesis of one-dimensional nanomaterials in seconds

06 August 2024, Version 1
This content is a preprint and has not undergone peer review at the time of posting.

Abstract

Rapid Joule heating (RJH) has shown its great power and rapid development in the synthesis of nanomaterials due to its simple procedure and extremely high reaction speed and energy efficiency. However, the morphology and structure controllable RJH preparation, for instance, the synthesis of one-dimensional (1D) nanomaterials, is still challenging. Inspired by the widely recognized vapor-liquid-solid (VLS) mechanism in many high temperature synthesis pathways, we develop a catalyzed RJH route for the synthesis of 1D nanomaterials. By introducing suitable metal catalysts, nanowires of refractory carbides, high entropy carbides, II-VI and III-V group semiconductors, as well as multi-walled and single-walled carbon nanotubes are catalytic grown in seconds. With a general applicability to various material types, a short synthesis time and a low energy consumption of kilojoules per gram of nanomaterials, this strategy presents great potential in material synthesis and production.

Keywords

Rapid Joule heating
1D nanomaterials
catalytic growth
Vapor-Liquid-Solid
carbon nanotubes

Supplementary materials

Title
Description
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Title
Catalytic synthesis of one-dimensional nanomaterials in seconds
Description
Supplementary Fig. 1 to S22, Tables S1 to S2.
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