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Bis(N-tert-butylacetamido)(dimethylamido)(chloro)titanium

01 March 2024, Version 2
Working Paper
This content is a preprint and has not undergone peer review at the time of posting.

Abstract

The titanium amidate compound bis(N-tert-butylacetamido)(dimethylamido)(chloro)titanium was synthesized by protonolysis of tris(dimethylamido)(chloro)titanium and was structurally characterized by 1H and 13C NMR spectrosocpy as well as X-ray diffraction. The compound does not appear to react cleanly nor readily with routine alkylating agents such as sec-butyllithium, benzyl potassium, or trimethylsilyl methyllithium.

Keywords

titanium
amidate

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Version History

Mar 01, 2024 Version 2

Version Notes

Updates with peer review

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The content is available under CC BY NC ND 4.0 [opens in a new tab]

DOI

10.26434/chemrxiv-2024-44g3f-v2
D O I: 10.26434/chemrxiv-2024-44g3f-v2 [opens in a new tab]

Funding

National Science Foundation
CHE-2101766

Author’s competing interest statement

The author(s) have declared they have no conflict of interest with regard to this content

Ethics

The author(s) have declared ethics committee/IRB approval is not relevant to this content

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