A simple setup miniaturisation with multiple benefits for Green Chemistry in nanoparticle synthesis

08 October 2021, Version 1
This content is a preprint and has not undergone peer review at the time of posting.

Abstract

The development of nanomaterials often relies on wet-chemical syntheses performed in reflux setups using round-bottom-flasks. An alternative approach to synthesise nanomaterials is presented that uses glass tubes designed for NMR analysis as reactors. It uses less solvent, generates less waste, provides safer conditions, is less prone to contamination and is compatible with high throughput screening.

Keywords

Green Chemistry
Nanoparticles
Synthesis
Miniaturisation
High throughput
Energy
Pair distribution function
NMR
Mini-reactors

Supplementary materials

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SI for A simple setup miniaturisation with multiple benefits for Green Chemistry in nanoparticle synthesis
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Experimental procedures, pictures, TEM and PDF data
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