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A General Method for Synthesis of Isomaleimide Derivatives

16 September 2021, Version 1
Working Paper
This content is a preprint and has not undergone peer review at the time of posting.

Abstract

A mild and efficient method for the synthesis of isoimide by a simple reaction of 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride (EDC) with various kinds of maleimicacid, succimicacid, pthaleimicacid in dichloromethane at room temperature is described.

Supplementary materials

Title
Description
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Title
Bis-isomaleimide experimental,
Description
Bis-isomaleimide experimental details with input of spectral values
Actions
Title
Bis-iso-maleimide spectral data
Description
Bis-iso-maleimide spectral data, H, C, and Ft-IR and EA of products. THe starting material and impurities are also included
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Version History

Sep 16, 2021 Version 1

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License

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The content is available under CC BY 4.0 [opens in a new tab]

DOI

10.26434/chemrxiv-2021-hb4dq
D O I: 10.26434/chemrxiv-2021-hb4dq [opens in a new tab]

Funding

S.R.G is thankful to Prof. Brent Sumerlin, SMU for supporting in the form of post-doctoral associate fellowship during January-2006 to December-2007 and allowing to work on this work.

Author’s competing interest statement

The author(s) have declared they have no conflict of interest with regard to this content

Ethics

The author(s) declare that they have sought and gained approval from the relevant ethics committee/IRB for this research and its publication.

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