Organic Chemistry

Synthesis of Chain Transfer Agents for RAFT Polymerization by using DBU

Authors

Abstract

Trithiocarbonate TTC, Dithioester DT containing RAFT chain transfer acid agents are efficiently and conveniently esterified by DBU. The significance of the reaction is mild reaction condition, high yield, easy simple workup, and reduction of reaction time. This protocol providing a useful alternative method for ester synthesis and makes the process very viable or more economic.

Content

Thumbnail image of DBU esterification manuscript-ready to send chemxiv.pdf

Supplementary material

Thumbnail image of DBU-esterification, Experimental-ready to send chemrxiv.pdf
SRGondi-DBU experimental part
DBU experimental details with in put of spectral values
Thumbnail image of DBU-esterfication-spectral data-ready to send chemrxiv.pdf
DBU-esterfication-spectral data
DBU spectral data with numbering of the compounds along with starting materials