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Intercalates of Bi2Se3 Studied in Situ by Time-Resolved Powder X-ray Diffraction and Neutron Diffraction

07 October 2020, Version 1
Working Paper
This content is a preprint and has not undergone peer review at the time of posting.

Abstract

Intercalation of lithium and ammonia into the layered semiconductor Bi2Se3 proceeds via a
hyperextended (by > 60 %) ammonia-rich intercalate, to eventually produce a layered compound
with lithium amide intercalated between the bismuth selenide layers which offer scope for further
chemical manipulation.

Keywords

intercalation
in situ diffraction
neutron diffracion
Bi2Se3

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Version History

Oct 07, 2020 Version 1

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The content is available under CC BY NC ND 4.0 [opens in a new tab]

DOI

10.26434/chemrxiv.13060565.v1
D O I: 10.26434/chemrxiv.13060565.v1 [opens in a new tab]

Funding

Netherlands Organisation for Scientific Research
019.181EN.003
Chemical Tuning of Layered Solids: Making the “Perfect Sandwich”.
https://app.dimensions.ai/details/grant/grant.7606044 [opens in a new tab]
European Commission
658832
Soft Chemical Control of the Physical Properties of Layered Solids
https://app.dimensions.ai/details/grant/grant.3939210 [opens in a new tab]
Engineering and Physical Sciences Research Council
EP/R042594/1
A SQUID Magnetometer for Quantum Materials, superconductors, molecular magnets and excited states
https://app.dimensions.ai/details/grant/grant.7612152 [opens in a new tab]
Engineering and Physical Sciences Research Council
EP/P018874/1
Soft chemical control to achieve new layered architectures and strongly correlated states.
https://app.dimensions.ai/details/grant/grant.6621479 [opens in a new tab]
Engineering and Physical Sciences Research Council
EP/M020517/1
Oxford Quantum Materials Platform Grant
https://app.dimensions.ai/details/grant/grant.3958654 [opens in a new tab]

Author’s competing interest statement

No conflicts of interest

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