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Abstract
We have developed an iron(III) chloride hexahydrate catalyzed formal [3+2] cycloaddition of tetrahydroisoquinolines with amide group-bearing Morita-Baylis-Hillman (MBH) carbonates. A range of highly functionalized dihydropyrrolo[2,1-a]isoquinolines could be prepared through SN2’/oxidation/ electrocyclization/aromatization cascade (32-62% yield).
Content
download asset Chemrxiv--20200321--FeCl3--3plus2--3.pdf 1 MB [opens in a new tab] cloud_download
pdf : 1 MB
Supplementary material
download asset 191118CHL_0m.txt 0.46 MB [opens in a new tab] cloud_download
txt : 0.46 MB
191118CHL 0m
