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Rapid and Mild Synthesis of Au-NHC Complexes in a Simple Two-Phase Flow Reactor

preprint
revised on 26.04.2021, 09:02 and posted on 27.04.2021, 06:09 by Helgi Freyr Jónsson, Anne Fiksdahl, Andrew Harvie

We describe a simple two-phase flow reactor which allows for the efficient and rapid synthesis of several Au(I)-NHC complexes under mild conditions, with minimal workup, and avoiding common problems with decomposition to Au(0). An optional second stage allows for direct synthesis of Au(III)-NHC complexes, without isolation of the Au(I)-NHC intermediate.

History

Email Address of Submitting Author

andrew.j.harvie@ntnu.no

Institution

NTNU

Country

Norway

ORCID For Submitting Author

0000-0002-7840-6639

Declaration of Conflict of Interest

The authors declare no conflicts of interest.

Version Notes

Version 2 uploaded with expanded methods

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