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NMR-Enhanced Crystallography Aids Open Metal-Organic Framework Discovery Using Solvent-Free Accelerated Aging

preprint
submitted on 16.06.2019 and posted on 17.06.2019 by Christopher A. O’Keefe, Cristina Mottillo, László Fábián, Tomislav Friscic, Robert W. Schurko
NMR-enhanced crystallography enables the characterization of a novel cadmium-based, open metal-organic framework (MOF) from a solvent-free "accelerated aging" process. Whereas accelerated aging was devised as a clean, mild route for making MOFs, these results highlight how it application in materials discovery and characterization is aided by a combination of X-ray diffraction and solid-state NMR spectroscopy.

Funding

NSERC Discovery Grant (RGPIN-2017-06467)

E. W. R. Steacie Memorial Fellowship (SMFSU 507347-17)

History

Email Address of Submitting Author

tomislav.friscic@mcgill.ca

Institution

McGill University

Country

Canada

ORCID For Submitting Author

0000-0002-3921-7915

Declaration of Conflict of Interest

We declare no conflict of interest.

Version Notes

This is version 1.

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